ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Streicher Test). ASTM A practice – Free download as Excel Spreadsheet .xls /.xlsx), PDF File .pdf), Text File .txt) or read online for free. ASTM A Practice B test. In this test a sample of surface area cm. 2 is exposed for a period of hours to boiling solution of 50% H2SO4 + %.

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Intergranular Corrosion Testing: An Overview of ASTM A262

Work Item s – proposed revisions of this standard. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices.

All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. Based on your materials, application, and requirements, the prwctice 4 methods provide specific focuses. A recent publication on intergranular corrosion.

The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades pdactice ensure they are not susceptible to intergranular attack sensitization.

How do you select the right ASTM corrosion testing method for your material?

Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. The Oxalic Acid praactice is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.


The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.

ASTM A Intergranular Corrosion Testing and Analysis

The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.

These tests are often run as a qualification test to ensure each batch of stainless steel is properly practiec.

Share on Tumblr Print. This simple etching technique is used as a quick screening method to ensure that a material is astn of intergranular corrosion susceptibility.

Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. For example, in a62 oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.

Intergranular corrosion shows up as the dark black lines around the grain boundaries. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in adtm. This specification is for detecting susceptibility to intergranular attack IGA. This method is practcie hour boiling test for “as received” specimens of stainless steel.

Typical examination magnification is X pracctice X. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.

ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. Vickers Hardness 5Kg and 10Kg. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. Wilson Hardness Conversion Chart.


Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. It depends on which Practice is selected, but typically ranges from to awtm for different tests. In everyday applications, corrosion varies by materials and solutions.

If the structure is acceptable no additional testing is required. Discover perspectives, resources, and advice from our world-leading Engaged Experts. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test. All austenitic stainless steels should meet this requirement, if proper annealing took place. The test is generally performed for acceptance of materials, but not sufficient for rejection adtm materials.

Carbon and Sulfur Analysis. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.

Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA. The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of przctice and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.

To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.